LIGHT SCATTERING OF POLYSACCHARIDE FROM LACQUER IN AQUEOUS SOLUTION
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LIGHT SCATTERING OF POLYSACCHARIDE FROM LACQUER IN AQUEOUS SOLUTION
Vol. 7, Issue 3, Pages: 252-257(1989)
Affiliations:
1. Department of Chamistry, Wuhan University, Wuhan) KUMANOTANI JU
2. Wuhan University
3. Wuhan
4. Faculty of Engineering
5. Ehime University
6. Japan
Author bio:
Funds:
DOI:
CLC:
Published:20 September 1989
Accepted:
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[1]张俐娜,杜予民,KUMANOTANI JU.LIGHT SCATTERING OF POLYSACCHARIDE FROM LACQUER IN AQUEOUS SOLUTION[J].Chinese Journal of Polymer Science,1989,{4}(03):252-257.
ZHANG Lina, DU Yumin, KUMANOTANI JU. LIGHT SCATTERING OF POLYSACCHARIDE FROM LACQUER IN AQUEOUS SOLUTION[J]. 1989, 7(3): 252-257.
[1]张俐娜,杜予民,KUMANOTANI JU.LIGHT SCATTERING OF POLYSACCHARIDE FROM LACQUER IN AQUEOUS SOLUTION[J].Chinese Journal of Polymer Science,1989,{4}(03):252-257.DOI:
ZHANG Lina, DU Yumin, KUMANOTANI JU. LIGHT SCATTERING OF POLYSACCHARIDE FROM LACQUER IN AQUEOUS SOLUTION[J]. 1989, 7(3): 252-257.DOI:
LIGHT SCATTERING OF POLYSACCHARIDE FROM LACQUER IN AQUEOUS SOLUTION
The polysaccharide having weight-average molecular weight M
w
=1. 09×10
5
isolated from the sap of lac trees (Vietnam)
was separated into 12 fractions by aqueous-phase preparative gel permeation chromatography. The molecular weights and molecular weight distributions of the fractions were measured in aqueous 0.08M KCl/0.01 M NaAc and 0.4M KCl/0.05M NaAc at pH =7. 6 by light scattering
viscometry and gel permeation chromatography. The Mark-Houwink equation in aqueous 0.08M KCl/0.01M NaAc at 30℃was found to be [η]= 2.28×10
-2
M
w
0.52
(cm
3
/g)
which indicated the polysaccharide chain in the aqueous solution to be a spherical random coil.
Abstract
The polysaccharide having weight-average molecular weight M
w
=1. 09×10
5
isolated from the sap of lac trees (Vietnam)
was separated into 12 fractions by aqueous-phase preparative gel permeation chromatography. The molecular weights and molecular weight distributions of the fractions were measured in aqueous 0.08M KCl/0.01 M NaAc and 0.4M KCl/0.05M NaAc at pH =7. 6 by light scattering
viscometry and gel permeation chromatography. The Mark-Houwink equation in aqueous 0.08M KCl/0.01M NaAc at 30℃ was found to be [η]= 2.28×10
-2
M
w
0.52
(cm
3
/g)
which indicated the polysaccharide chain in the aqueous solution to be a spherical random coil.
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