PREPARATION OF POLY（METHYL METHACRYLATE）/LAYERED DOUBLE HYDROXIDES NANOCOMPOSITES via in situ SOLUTION POLYMERIZATION

Ang-ran Wang Yong-zhong Bao~() Zhi-xue Weng Zhi-ming Huang State Key Laboratory of Chemical Engineering; Zhejiang University; Hangzhou 310027; China

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PREPARATION OF POLY（METHYL METHACRYLATE）/LAYERED DOUBLE HYDROXIDES NANOCOMPOSITES via in situ SOLUTION POLYMERIZATION

Updated：2021-06-21

- PREPARATION OF POLY（METHYL METHACRYLATE）/LAYERED DOUBLE HYDROXIDES NANOCOMPOSITES via in situ SOLUTION POLYMERIZATION
- Issue 6, Pages: 573-579(2007)
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  This work was supported by the Zhejiang Grant Science and Technology Program（No.2005C11039）.()
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Ang-ran Wang Yong-zhong Bao~() Zhi-xue Weng Zhi-ming Huang State Key Laboratory of Chemical Engineering, Zhejiang University, Hangzhou 310027, et al. PREPARATION OF POLY（METHYL METHACRYLATE）/LAYERED DOUBLE HYDROXIDES NANOCOMPOSITES via in situ SOLUTION POLYMERIZATION. [J]. (6):573-579(2007)
DOI：

Ang-ran Wang Yong-zhong Bao~() Zhi-xue Weng Zhi-ming Huang State Key Laboratory of Chemical Engineering, Zhejiang University, Hangzhou 310027, et al. PREPARATION OF POLY（METHYL METHACRYLATE）/LAYERED DOUBLE HYDROXIDES NANOCOMPOSITES via in situ SOLUTION POLYMERIZATION. [J]. (6):573-579(2007) DOI：

摘要

<正>An exfoliated layered double hydroxides/poly（methyl methacrylate）（LDHs/PMMA）nanocomposite was prepared by in situ solution polymerization of methyl methacrylate（MMA）in the presence of 4-vinylbenzenesulfonate intercalated LDHs（MgAl-VBS LDHs）.MgAl-VBS LDHs was prepared by the ion exchange method,and the structure and composition of the MgA1-VBS LDHs were determined by X-ray diffraction（XRD）,infrared spectroscopy and elemental analysis.XRD and transmission electron microscopy（TEM）were employed to examine the structure of LDHs/PMMA nanocomposite.It was indicated that the LDHs layers were well exfoliated and dispersed in the PMMA matrix.The grafting of PMMA onto LDHs was confirmed by the extraction result and the weight fraction of grafted PMMA increased as the weight fraction of LDHs in the nanocomposites increased.

Abstract

An exfoliated layered double hydroxides/poly（methyl methacrylate）（LDHs/PMMA）nanocomposite was prepared by in situ solution polymerization of methyl methacrylate（MMA）in the presence of 4-vinylbenzenesulfonate intercalated LDHs（MgAl-VBS LDHs）.MgAl-VBS LDHs was prepared by the ion exchange method,and the structure and composition of the MgA1-VBS LDHs were determined by X-ray diffraction（XRD）,infrared spectroscopy and elemental analysis.XRD and transmission electron microscopy（TEM）were employed to examine the structure of LDHs/PMMA nanocomposite.It was indicated that the LDHs layers were well exfoliated and dispersed in the PMMA matrix.The grafting of PMMA onto LDHs was confirmed by the extraction result and the weight fraction of grafted PMMA increased as the weight fraction of LDHs in the nanocomposites increased.

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